MS Report from Instrument: LCMS-02 File ..1\\DATA\\2018\\20180709\\303\\BIZ2018-709-WYQ2.D Tgt Mass (CHM): Injection Date : 9 Jul 18 6:50 pm +0800 Seq. Line : 52 Sample Name : BIZ2018-709-WYQ2 Location : P1-B-04 Acq. Operator : LQ_1052 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\data\\2018\\20180709\\303\\1-POS-3MIN-1.M Analysis Method : D:\\CHEM32\\1\\DATA\\2018\\20180709\\303\\1-POS-3MIN-1.M Catalog No : HY-108463 Batch#31413 A-RP-314 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-314 Oven Temperature : 45 DAD1 B, Sig=214,4 Ref=off 1.9281.5061.6771.8821.9802.036mAU1500100050000.5 DAD1 C, Sig=254,4 Ref=off mAU20001.2181.5061.557100000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701500000100000050000000.511.5 Ion 208.1, MSD1 208.1,Target Mass 207.1 +H Positive, EIC=207.8:208.8 150000010000002.32750000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.5222.0282.5min11.51.92822.5min1.9752.0361.522.0282.5min2.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.51 0.01 3.07 3.87 0.14 235 1.68 0.01 4.67 5.42 0.22 235 1.88 0.01 9.81 10.47 0.46 235 1.93 0.02 2101.17 2286.13 98.66 235 1.98 0.01 5.98 7.74 0.28 208 2.04 0.01 5.11 6.48 0.24 208 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.22 0.01 0.95 1.41 0.03 235 1.51 0.01 0.65 0.85 0.02 235 1.56 0.01 1.15 1.50 0.04 235 1.93 0.02 2934.68 2829.28 99.42 235 1.98 0.02 11.27 12.10 0.38 208 2.04 0.01 3.15 4.12 0.11 208 Integration Results for MSD1 TIC, MS FileLCMS-02 7/10/2018 13:49:39 LQ_1052
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MS Report from Instrument: LCMS-02
RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 2.03 0.05 7221596.50 1977604.13 100.00 208LCMS-02 7/10/2018 13:49:39 LQ_1052
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MS Report from Instrument: LCMS-02
Ret. Time: 2.03 <<<< POSITIVE SPECTRA >>>> ES-API Positive350000300000250000200000150000100000500000200300400500600700800900m/z 209.2 208.2LCMS-02 7/10/2018 13:49:39 LQ_1052
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