MS Report from Instrument: LCMS-02 File ..6-1 2017-07-06 15-14-20\\CPK2017-706-12654.D Tgt Mass (CHM): Injection Date : 6 Jul 17 7:02 pm +0800 Seq. Line : 49 Sample Name : CPK2017-706-12654 Location : P1-D-09 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\chem32\\1\\DATA\\20170706\\20170706-1 2017-07-06 15-14-20\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\DATA\\20170706\\20170706-1 2017-07-06 15-14-20\\1-POS-3MIN.M Catalog No : HY-15192 Batch#12654 A-RP-186 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 B, Sig=214,4 Ref=off mAU1500100050000.5 DAD1 C, Sig=254,4 Ref=off mAU4001.2431.6041.77820000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701500001000005000000.511.5 Ion 383.5, MSD1 383.5,Target Mass 382.5 +H Positive, EIC=383.2:384.2 1500001000005000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min1.96122.5min1.9330.7101.5912.03311.51.93322.5min2.0541.51.96222.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.71 0.03 12.13 5.97 1.29 157 1.59 0.02 1.04 0.91 0.11 ND 1.93 0.03 924.90 614.61 98.57 383 2.03 0.01 0.21 0.39 0.02 383 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.24 0.04 0.96 0.78 0.11 432 1.60 0.16 1.48 0.79 0.17 ND 1.78 0.06 1.28 0.57 0.15 ND 1.93 0.03 863.75 572.62 99.38 383 2.05 0.12 1.68 -0.05 0.19 233 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------|LCMS-02 7/7/2017 9:29:32 ZLJ_587Page 1 of 3
MS Report from Instrument: LCMS-02 1.96 0.03 375814.25 173621.38 100.00 383LCMS-02 7/7/2017 9:29:32 ZLJ_587Page 2 of 3
MS Report from Instrument: LCMS-02Ret. Time: 1.96 <<<< POSITIVE SPECTRA >>>> ES-API Positive35000300002500020000 384.1150001000050000200300400500600700800900m/z 383.2LCMS-02 7/7/2017 9:29:32 ZLJ_587Page 3 of 3
